Laboratory schedule

Fall 2009

go directly to list of open lab slots
go directly to lab schedule

Laboratory work will count for 20% of your final grade. You are required to complete all experiments; makeup time is provided during the last week of the term. Unexcused absences from lab will not be made up.

All exercises require that something be returned for grading; most experiments will require formal reports, which will be submitted in a standard format. Reports will be graded with a standard rubric.

Students who must miss a laboratory period are still responsible for the techniques and ideas dealt with in that experiment. Note that weeks 11 and 12 comprise a single experiment.

"Trading lab periods" is acceptable and prior instructor approval is not required (though you must notify the instructor). You may trade with another student, or use one of the open lab slots shown below. Open laboratory slots will be made available to students from other sections on a first-come, first-served basis.

Day and time Openings
Section 1 2-5 PM T 0
Section 2 3-6 PM W 0
Section 3 8-11 AM R 3
Section 4 2-5 PM R 1

The instructor must be informed of trades and rescheduling in advance so that proper preparations can be made.

Week Lab dates Experiments Related textbook material You must hand in...
1 Sept 1-3 Introduction to the laboratory; "Safety in the organic chemical laboratory" (TECH 700) Shoker map; fire extinguishers; introduction to molecular model kits   Contract at end of lab; TECH 700 worksheet due Week 2
2 Sep 8-10 "Measuring the melting points of compounds and mixtures" (TECH 701); work with model kits continues from last week   Prelab; modeling worksheets at end of lab; post-lab worksheet Week 3
3 Sep 15-17 Isolation of caffeine see the Separatory Funnel video Prelab; Report, Week 4
4 Sep 22-24 Molecular modeling exercises
with model kit and ArgusLab
  worksheets as assigned
5 Sep 29-Oct 1 Model kit exercise; Introduction to polarimeter; Resolution of a racemic mixture, Week 1 5.8-5.10, 5.16 Prelab; worksheets at end of lab period
6 Oct 6-8
Fall Break
Exercises TBA   as assigned
7 Oct 13-15 Resolution of a racemic mixture, Week 2 Chapter 5 Prelab; Report, Week 8
8 Oct 20-22 Thin-layer chromatography (TLC)   Prelab; Report, Week 9
9 Oct 27-29 Dehydration of an alcohol 10.4 Prelab; Report, Week 10
10 Nov 3-5 Analysis of fatty acids 16.11, 16.12 Prelab; report, week 11
11 Nov 10-12 Reduction of a ketone 17.6 Prelab; Report, Week 12
12 Nov 17-19 Saponification 16.11, 16.12 Prelab; Report, Week 13
14 Nov 24-26 No Laboratory (Thanksgiving)    
13 Dec 1-3 Laboratory Final Exam
makeup work TBA
  worth two reports
15 Dec 8-10 makeup work TBA