Laboratory schedule

Fall 2010

go directly to list of open lab slots
go directly to lab schedule

Laboratory work will count for 20% of your final grade. You are required to complete all experiments; makeup time is provided during the last week of the term. Unexcused absences from lab will not be made up.

All exercises require that something be returned for grading; most experiments will require formal reports, which will be submitted in a standard format. Reports will be graded with a standard rubric.

Students who must miss a laboratory period are still responsible for the techniques and ideas dealt with in that experiment. Note that weeks 11 and 12 comprise a single experiment.

"Trading lab periods" is acceptable and prior instructor approval is not required (though you must notify the instructor). You may trade with another student, or use one of the open lab slots shown below. Open laboratory slots will be made available to students from other sections on a first-come, first-served basis.

Day and time Openings
Section 1 2-5 PM T 0
Section 2 2-5 PM W 0
Section 3 8-11 AM R 1
Section 4 2-5 PM R 0
Section 5 2-5 PM M 0

The instructor must be informed of trades and rescheduling in advance so that proper preparations can be made.

Week Lab dates Experiments Related textbook material You must hand in...
1 Aug 30-Sept 2 Introduction to the laboratory; "Safety in the organic chemical laboratory" (TECH 700) Shoker map; fire extinguishers; introduction to molecular model kits   Contract at end of lab; TECH 700 worksheet due Week 2
2 Sep 6-9 "Biosynthesis of ethanol" (page 54), week 1; TECH 701 "Measuring the melting points of compounds and mixtures"   Prelab for TECH 701; Postlab for TECH 701 due
3 Sep 13-16 Biosynthesis of ethanol, week 2   Prelab for Biosynthesis of ethanol; Report, Week 4
4 Sep 20-23 Molecular modeling exercises
with model kit and ArgusLab
  worksheets as assigned
5 Sep 27-30 Resolution of a racemic mixture, Week 1
Introduction to the polarimeter
5.8-5.10, 5.16 Prelab; worksheets at end of lab period
6 Oct 4-7
Fall Break
Exercises TBA   as assigned
7 Oct 11-14 Resolution of a racemic mixture, Week 2 Chapter 5; how to use a separatory funnel Prelab; Report, Week 8
8 Oct 18-21 Thin-layer chromatography (TLC)   Prelab; Report, Week 9
9 Oct 25-28 Dehydration of an alcohol
Week changed!
10.4 Prelab; Report, Week 10
10 Nov 1-4 Reduction of a ketone
Week changed!
17.6 Prelab; report, week 11 12
Week changed!
11 Nov 8-11 Multistep synthesis of triphenylmethanol, week 1 16.11, 16.15 Prelab
12 Nov 15-18 Multistep synthesis of triphenylmethanol, week 2 10.12, 17.4 Prelab
13 Nov 22-25 No Laboratory (Thanksgiving)    
14 Nov 29-Dec 2 Laboratory Final Exam
recrystallize triphenylmethanol
  Report for multistep synthesis due Dec 10
15 Dec 6-9 makeup work TBA